N,S-substituted nitrodienes from naphthylthiosubstituted nitrodienes and S-, S,S-substituted dienes from hexachloro-1,3-butadiene


Ibis C., Gokmen Z.

PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, cilt.182, sa.5, ss.1053-1059, 2007 (SCI İndekslerine Giren Dergi) identifier identifier

  • Cilt numarası: 182 Konu: 5
  • Basım Tarihi: 2007
  • Doi Numarası: 10.1080/10426500601093838
  • Dergi Adı: PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS
  • Sayfa Sayıları: ss.1053-1059

Özet

Mono(thio)substituted dienes 1 gave compounds 3a-c, 7, 9, and 11 on reaction with pipe-razine derivatives in dry ether. N,S-substituted nitrodiene 5 was obtained from the reaction of 1 with 1,4-dioxospriol 4. Hexachlorobutadiene 12 in a water-ethanol mixture in the presence of sodium hydroxide reacted with ethyleneglycol bismercaptoacetate 13 to give thiosubstituted thioethers 14 and 15.