New thio-substituted butadiene and butenyne compounds from hexachlorobutenes and thiols


Ibis C., Bal T.

PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, cilt.178, ss.431-438, 2003 (SCI İndekslerine Giren Dergi) identifier identifier

  • Cilt numarası: 178 Konu: 3
  • Basım Tarihi: 2003
  • Doi Numarası: 10.1080/10426500307913
  • Dergi Adı: PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS
  • Sayfa Sayıları: ss.431-438

Özet

2,3-Di-H-butene compound 1 gave compounds 3a-f, 4a, 4e, and 5a-d in the presence of thiols 2a-f and Et3N (or NaOH). Compound 7e was obtained from the reaction of 1,3-Di-H-butene 6 with naphthylthiol in DMF In the presence of NaOH, compound 6 and 2 mmol of thiol 2g in EtOHgave compounds 8, 9, 10, and 11.